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{
"count": 97,
"next": "http://glycodata.org/api/gdd/polymer-solubility/?format=api&page=5",
"previous": "http://glycodata.org/api/gdd/polymer-solubility/?format=api&page=3",
"results": [
{
"id": 61,
"polymer": "Dextran",
"solvent": "Cyclohexane",
"concentration_mg_ml": "15.11",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "27",
"transmission_25C": "23",
"transmission_60C": "18",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.11 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.11 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.5 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=210); observed range 15-33 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Cyclohexane at 15.11 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 62,
"polymer": "Dextran",
"solvent": "Cyclohexanone",
"concentration_mg_ml": "5.02",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "22",
"transmission_25C": "22",
"transmission_60C": "22",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "5.02 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 5.02 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.8 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=210); observed range 19-25 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Cyclohexanone at 5.02 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 63,
"polymer": "Dextran",
"solvent": "Cyclohexanone",
"concentration_mg_ml": "50",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "0",
"transmission_25C": "0",
"transmission_60C": "0",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "50 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 50 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.8 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 0-0 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Cyclohexanone at 50 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 64,
"polymer": "Dextran",
"solvent": "Cyclopentanone",
"concentration_mg_ml": "15.03",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "2",
"transmission_25C": "1",
"transmission_60C": "1",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.03 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.03 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 1-2 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Cyclopentanone at 15.03 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 65,
"polymer": "Dextran",
"solvent": "DMAc",
"concentration_mg_ml": "14.71",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "77",
"transmission_25C": "61",
"transmission_60C": "",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.71 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.71 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=90); observed range 53-83 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in DMAc at 14.71 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 66,
"polymer": "Dextran",
"solvent": "DMF",
"concentration_mg_ml": "49.54",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "81",
"transmission_25C": "63",
"transmission_60C": "58",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "49.54 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 49.54 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.8 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=155); observed range 15-99 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in DMF at 49.54 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 67,
"polymer": "Dextran",
"solvent": "DMF",
"concentration_mg_ml": "5.39",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "100",
"transmission_25C": "71",
"transmission_60C": "100",
"cloud_point_C": "44",
"method": "Experiment",
"conditions": "5.39 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 5.39 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.8 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=83); observed range 55-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in DMF at 5.39 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Approx. cloud point on cooling ~44 °C. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 68,
"polymer": "Dextran",
"solvent": "DMSO",
"concentration_mg_ml": "14.66",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "43",
"transmission_25C": "100",
"transmission_60C": "100",
"cloud_point_C": "18",
"method": "Experiment",
"conditions": "14.66 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.66 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.9 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=49); observed range 0-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in DMSO at 14.66 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Approx. cloud point on cooling ~18 °C. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 69,
"polymer": "Dextran",
"solvent": "DMSO",
"concentration_mg_ml": "4.96",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "0",
"transmission_25C": "100",
"transmission_60C": "100",
"cloud_point_C": "22",
"method": "Experiment",
"conditions": "4.96 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 4.96 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.9 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=52); observed range 0-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in DMSO at 4.96 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Approx. cloud point on cooling ~22 °C. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 70,
"polymer": "Dextran",
"solvent": "DMSO",
"concentration_mg_ml": "50.03",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "0",
"transmission_25C": "100",
"transmission_60C": "100",
"cloud_point_C": "21",
"method": "Experiment",
"conditions": "50.03 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 50.03 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.9 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=47); observed range 0-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in DMSO at 50.03 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Approx. cloud point on cooling ~21 °C. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 71,
"polymer": "Dextran",
"solvent": "Diethyl ether",
"concentration_mg_ml": "15.03",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "0",
"transmission_25C": "0",
"transmission_60C": "0",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.03 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.03 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.8 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 0-0 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Diethyl ether at 15.03 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 72,
"polymer": "Dextran",
"solvent": "Ethyl acetate",
"concentration_mg_ml": "14.54",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "0",
"transmission_25C": "0",
"transmission_60C": "0",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.54 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.54 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.5 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 0-0 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Ethyl acetate at 14.54 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 73,
"polymer": "Dextran",
"solvent": "Ethyl lactate",
"concentration_mg_ml": "15.07",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "1",
"transmission_25C": "1",
"transmission_60C": "1",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.07 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.07 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 98 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 1-1 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Ethyl lactate at 15.07 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 74,
"polymer": "Dextran",
"solvent": "Formamide",
"concentration_mg_ml": "15.02",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Soluble",
"transmission_10C": "100",
"transmission_25C": "100",
"transmission_60C": "100",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.02 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.02 mg/mL polymer, Mn 9000-10000 g/mol (Sigma). Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 98-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Formamide at 15.02 mg/mL is soluble: clear (T > 85 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 75,
"polymer": "Dextran",
"solvent": "Heptane",
"concentration_mg_ml": "15.05",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "47",
"transmission_25C": "38",
"transmission_60C": "26",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.05 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.05 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=211); observed range 15-59 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Heptane at 15.05 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 76,
"polymer": "Dextran",
"solvent": "Isobutyl acetate",
"concentration_mg_ml": "14.9",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "2",
"transmission_25C": "2",
"transmission_60C": "3",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.9 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.9 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=50); observed range 2-4 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Isobutyl acetate at 14.9 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 77,
"polymer": "Dextran",
"solvent": "NMP",
"concentration_mg_ml": "15.2",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "100",
"transmission_25C": "61",
"transmission_60C": "63",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.2 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.2 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=93); observed range 39-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in NMP at 15.2 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 78,
"polymer": "Dextran",
"solvent": "NMP",
"concentration_mg_ml": "5",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "100",
"transmission_25C": "58",
"transmission_60C": "100",
"cloud_point_C": "59",
"method": "Experiment",
"conditions": "5 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 5 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=131); observed range 41-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in NMP at 5 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Approx. cloud point on cooling ~59 °C. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 79,
"polymer": "Dextran",
"solvent": "NMP",
"concentration_mg_ml": "50.01",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "100",
"transmission_25C": "68",
"transmission_60C": "65",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "50.01 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 50.01 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=106); observed range 26-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in NMP at 50.01 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 80,
"polymer": "Dextran",
"solvent": "Pentane",
"concentration_mg_ml": "14.99",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "36",
"transmission_25C": "39",
"transmission_60C": "22",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.99 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.99 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 98 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=160); observed range 10-48 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Pentane at 14.99 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
}
]
}