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{
"count": 97,
"next": "http://glycodata.org/api/gdd/polymer-solubility/?format=api&page=4",
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"results": [
{
"id": 41,
"polymer": "Chitosan",
"solvent": "Formamide",
"concentration_mg_ml": "14.99",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Insoluble",
"transmission_10C": "1",
"transmission_25C": "2",
"transmission_60C": "2",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.99 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.99 mg/mL polymer, Mn 15000 g/mol (Polysciences). Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 1-5 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in Formamide at 14.99 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 42,
"polymer": "Chitosan",
"solvent": "Heptane",
"concentration_mg_ml": "15.02",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Insoluble",
"transmission_10C": "3",
"transmission_25C": "4",
"transmission_60C": "4",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.02 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.02 mg/mL polymer, Mn 15000 g/mol (Polysciences); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=50); observed range 3-4 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in Heptane at 15.02 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 43,
"polymer": "Chitosan",
"solvent": "Isobutyl acetate",
"concentration_mg_ml": "14.9",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Insoluble",
"transmission_10C": "1",
"transmission_25C": "1",
"transmission_60C": "1",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.9 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.9 mg/mL polymer, Mn 15000 g/mol (Polysciences); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=50); observed range 1-1 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in Isobutyl acetate at 14.9 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 44,
"polymer": "Chitosan",
"solvent": "Petroleum ether",
"concentration_mg_ml": "14.94",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Insoluble",
"transmission_10C": "3",
"transmission_25C": "4",
"transmission_60C": "5",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.94 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.94 mg/mL polymer, Mn 15000 g/mol (Polysciences). Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 3-5 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in Petroleum ether at 14.94 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 45,
"polymer": "Chitosan",
"solvent": "Pyridine",
"concentration_mg_ml": "15.72",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Partially soluble",
"transmission_10C": "21",
"transmission_25C": "16",
"transmission_60C": "10",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.72 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.72 mg/mL polymer, Mn 15000 g/mol (Polysciences); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=202); observed range 10-21 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in Pyridine at 15.72 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 46,
"polymer": "Chitosan",
"solvent": "Carbon disulfide",
"concentration_mg_ml": "14.97",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Partially soluble",
"transmission_10C": "11",
"transmission_25C": "13",
"transmission_60C": "27",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.97 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.97 mg/mL polymer, Mn 15000 g/mol (Polysciences); solvent purity 99.5 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=210); observed range 11-28 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in Carbon disulfide at 14.97 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 47,
"polymer": "Chitosan",
"solvent": "m-cresol",
"concentration_mg_ml": "15.14",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Partially soluble",
"transmission_10C": "",
"transmission_25C": "50",
"transmission_60C": "44",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.14 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.14 mg/mL polymer, Mn 15000 g/mol (Polysciences); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=184); observed range 44-84 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in m-cresol at 15.14 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 48,
"polymer": "Chitosan",
"solvent": "n-Butanol",
"concentration_mg_ml": "49.97",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Insoluble",
"transmission_10C": "0",
"transmission_25C": "0",
"transmission_60C": "0",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "49.97 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 49.97 mg/mL polymer, Mn 15000 g/mol (Polysciences); solvent purity 99.4 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 0-0 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in n-Butanol at 49.97 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 49,
"polymer": "Chitosan",
"solvent": "n-Butanol",
"concentration_mg_ml": "5.22",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Partially soluble",
"transmission_10C": "9",
"transmission_25C": "10",
"transmission_60C": "12",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "5.22 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 5.22 mg/mL polymer, Mn 15000 g/mol (Polysciences); solvent purity 99.4 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=194); observed range 9-13 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in n-Butanol at 5.22 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 50,
"polymer": "Chitosan",
"solvent": "Styrene",
"concentration_mg_ml": "14.92",
"molecular_weight": "15000",
"supplier": "Polysciences",
"solubility_class": "Partially soluble",
"transmission_10C": "48",
"transmission_25C": "66",
"transmission_60C": "49",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.92 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.92 mg/mL polymer, Mn 15000 g/mol (Polysciences). Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=210); observed range 48-71 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Chitosan in Styrene at 14.92 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 51,
"polymer": "Dextran",
"solvent": "1,4-dioxane",
"concentration_mg_ml": "14.9",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "0",
"transmission_25C": "2",
"transmission_60C": "1",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.9 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.9 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.8 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 0-2 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in 1,4-dioxane at 14.9 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 52,
"polymer": "Dextran",
"solvent": "1-Octanol",
"concentration_mg_ml": "15.02",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "1",
"transmission_25C": "2",
"transmission_60C": "2",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.02 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.02 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=53); observed range 1-59 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in 1-Octanol at 15.02 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 53,
"polymer": "Dextran",
"solvent": "2,4,6-trimethylpyridine",
"concentration_mg_ml": "15",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "12",
"transmission_25C": "9",
"transmission_60C": "2",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=77); observed range 2-12 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in 2,4,6-trimethylpyridine at 15 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 54,
"polymer": "Dextran",
"solvent": "2,4,6-trimethylpyridine",
"concentration_mg_ml": "15.04",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "13",
"transmission_25C": "9",
"transmission_60C": "3",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.04 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.04 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=78); observed range 3-13 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in 2,4,6-trimethylpyridine at 15.04 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 55,
"polymer": "Dextran",
"solvent": "Anisole",
"concentration_mg_ml": "14.31",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "",
"transmission_25C": "63",
"transmission_60C": "23",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.31 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.31 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=170); observed range 22-83 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Anisole at 14.31 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 56,
"polymer": "Dextran",
"solvent": "Benzene",
"concentration_mg_ml": "5.03",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "100",
"transmission_25C": "74",
"transmission_60C": "50",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "5.03 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 5.03 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=188); observed range 48-100 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Benzene at 5.03 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 57,
"polymer": "Dextran",
"solvent": "Benzene",
"concentration_mg_ml": "50.01",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "",
"transmission_25C": "9",
"transmission_60C": "1",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "50.01 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 50.01 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=47); observed range 1-10 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Benzene at 50.01 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 58,
"polymer": "Dextran",
"solvent": "Benzyl alcohol",
"concentration_mg_ml": "15.12",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "66",
"transmission_25C": "67",
"transmission_60C": "40",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "15.12 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 15.12 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=205); observed range 39-89 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Benzyl alcohol at 15.12 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 59,
"polymer": "Dextran",
"solvent": "Chlorobenzene",
"concentration_mg_ml": "14.89",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Partially soluble",
"transmission_10C": "",
"transmission_25C": "79",
"transmission_60C": "27",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.89 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.89 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=138); observed range 26-83 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Chlorobenzene at 14.89 mg/mL is partially soluble: transmission between 10 and 85 % at some temperature on cooling. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
},
{
"id": 60,
"polymer": "Dextran",
"solvent": "Chloroform",
"concentration_mg_ml": "14.9",
"molecular_weight": "9000-10000",
"supplier": "Sigma",
"solubility_class": "Insoluble",
"transmission_10C": "4",
"transmission_25C": "3",
"transmission_60C": "1",
"cloud_point_C": "",
"method": "Experiment",
"conditions": "14.9 mg/mL, 10-60 °C, 0.5 °C/min",
"conditions_detail": "Crystal16 turbidity (645 nm), cooling ramp 60 to 10 °C at 0.5 °C/min after two heat/cool cycles; holds 120 min at 10 °C and 60 min at 60 and 25 °C; stirring 900 rpm. Sample: 14.9 mg/mL polymer, Mn 9000-10000 g/mol (Sigma); solvent purity 99.8 %. Transmission binned per 1 °C (median of Savitzky-Golay filtered cooling-phase points, n=51); observed range 1-4 %. Class thresholds from the source paper: insoluble <10 %, soluble >85 %, partial 10-85 %. Nonequilibrium (0.5 °C/min).",
"doi": "10.1021/acs.jpcb.4c06500",
"comments": "Dextran in Chloroform at 14.9 mg/mL is insoluble: turbid (T < 10 %) over the whole 10-60 °C cooling ramp. Class refers to nonequilibrium behaviour during the cooling ramp, not thermodynamic solubility. Data: Amrihesari et al., J. Phys. Chem. B 2024 (github.com/mona2442/Polymer-Solubility-Data_Crystal16)."
}
]
}